Schumann, HerbertOpitz, Joachim2019-01-042019-01-0419800932-0776https://depositonce.tu-berlin.de/handle/11303/8804http://dx.doi.org/10.14279/depositonce-7933[(t-C4H9)3PH]2[{Ru(μI)I2(CO)[P(t-C4H9)2H]}2] is prepared by the reaction of RUC13 · (H2O)x with CO, NaI, and P(t-C4H9)3 in 2-methoxyethanol. Its IR, Raman, and NMR spectra are reported and discussed. [Ru(μ-I)(CO)2P(t-C4H9)2H)2 is obtained by the reaction of [Ru(μ-I)I(CO)3]2 with P(t-C4H9)3 in 2-methoxyethanol. The X18MAA′M′X′18 spin system of its 1H NMR spectrum is analysed.de540 Chemie und zugeordnete Wissenschaftenruthenium(i) complexdi-tert-butylphosphinenmr spectra;ruthenium(ii) complextri-tert-butylphosphonium saltArticle1865-7117